That temp/time i had mentioned previously has changed some. After several curing tests with different lead free stuff..... i now keep the temp and time as close to what the manufacture states as i can. 350* for around 20 minutes. I will add, after the initial cure, an xtra 10 minutes and drop the heat to 325* if i think it will not be totaly cured. I am using almost all CSI Pro-Tec powder as well.
Hawnjigs had given me a rough estimate at what the melt point was for his bismuth alloy mix and it was (if i remember right) above the cure temp fro Pro-Tec so i have raised my temp to 350* and have not had any problem.
Melt point for tin is ~450. What is the melt point of pure bismuth?
I do cure them in singles before i do a larger batch and test them after they come out of the oven to make sure they are cured good. A couple thumps on concrete and a knife blade pushed against the paint will tell if it is going to chip. If it chips...... back in the oven it goes.
One problem i have run into with some of the leadfree alloy heads i have, is when i am re-heating them to do a second color. If the head gets too hot it makes odd lumps push out from the metal. Metalic pimples is my best description. Only happens when i 're-heat' a jig TOO hot after it has one coat of paint on it already. Need to get some pics. of the zits.
whew - that was alot of typing.